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A Soft Chemistry Approach to Extended [Co6Se8] Materials

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자료유형	E-Book
개인저자	Champsaur, Anouck.
단체저자명	Columbia University. Chemistry.
서명/저자사항	A Soft Chemistry Approach to Extended [Co6Se8] Materials.
발행사항	[S.l.] : Columbia University., 2018
발행사항	Ann Arbor : ProQuest Dissertations & Theses, 2018
형태사항	184 p.
소장본 주기	School code: 0054.
ISBN	9780438149557
일반주기	Source: Dissertation Abstracts International, Volume: 79-11(E), Section: B. Adviser: Colin Nuckolls.
요약	This dissertation describes advances toward creating programmable building blocks and assembling them into new, tailored materials. I describe extended materials formed of bonded sets of cobalt selenide clusters. Rationally designed chemical tra
요약	The cobalt selenide clusters fundamental to this study are members of a larger class of clusters with the M6E8 core (M = metal, E = chalcogen). Chapter 1 introduces this family of clusters and reviews examples of previously made materials.
요약	Chapter 2 unveils a family of site-differentiated clusters, Co6 Se8(CO)x(PEt3)6-x, their substitution reactions, and assembly into bridged dimers and trimers. Electrochemical methods were used to investigate electronic coupling between the cores
요약	Chapter 3 introduces electrocrystallization as a method to synthesize extended, crystalline, solid state compounds from superatomic building blocks. By electrocrystallizing redox-active [Co6Se8] clusters with labile ligands in the presence of an
요약	Chapter 4 presents a metal coordination approach to [Co6Se 8] materials via reactive groups on the capping ligands. The redox-activity and multinuclearity of the superatom components creates a new level of complexity and synthetic sophistication
요약	Finally, Chapter 5 outlines a novel chemical transformation that dimerizes [Co6Se8] units to form a material with an expanded core, [Co12Se16], that exhibits electronic and optical properties distinct from the parent monomer. To accomplish this
요약	These chapters present novel synthetic approaches toward creating [Co 6Se8] materials with tuned dimensionality, size, and extensive charge delocalization.
일반주제명	Inorganic chemistry. Materials science. Chemistry.
언어	영어
기본자료 저록	Dissertation Abstracts International79-11B(E). Dissertation Abstract International
대출바로가기	http://www.riss.kr/pdu/ddodLink.do?id=T14999478